Journal of the Japan Institute of Metals and Materials
Online ISSN : 1880-6880
Print ISSN : 0021-4876
ISSN-L : 0021-4876
Electron-Microscopic Study on the Progress of Reduction of MoO3 Single Crystal (Electron-Microscopic Studies on the Progress of Reduction of Metal Oxides by Hydrogen, 2nd Report)
Ryuzo Ueda
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1959 Volume 23 Issue 5 Pages 292-295

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Abstract
Molybdenum trioxide crystals were mounted on the sharply pointed end of a fine tungsten wire and exposed to heated hydrogen gas under about one atmospheric pressure in the specimen-treating adaptor attached to the electron microscope, previously devised by the author and others, and the morphological and chemical changes in a certain chosen region of the specimen were followed by taking micrographs and selected-area electron-diffraction patterns. Many informations on the formation of molybdenum metal particles were obtained. The mechanism of formation of metallic particles is discussed.
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