Journal of the Japanese Association for Crystal Growth
Online ISSN : 2187-8366
Print ISSN : 0385-6275
ISSN-L : 0385-6275
Scavenging Technique for Crystal Growth of Calcium Fluoride(<Special Issue>Crystal Growth Technology of Fluoride and Oxide Developed from the Viewpoint of Their Material and Functional Properties)
Tomoru Oba
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2006 Volume 33 Issue 3 Pages 130-134

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Abstract
New scavenging method is designed to obtain calcium fluoride crystals which optical properties are excellent, eg. internal trans-mittance and laser durability. Reaction processes between scav-engers and raw material are examined by degas analyzing during heating. The results suggest the simple method that raw material with scavenger is heated in vacuum atmosphere is not enough to make scavenging process progress completely. Then, two steps are applied. The first step, scavenging reaction progess in inert gas atmosphere during the heating process. And the second step, degas of remained scavenger and reaction products progress in vacuum atmosphere. Using this method, optical properties of cal-cium fluoride crystals improved very much.
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© 2006 The Japanese Association for Crystal Growth
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