2017 年 64 巻 12 号 p. 677-680
Carbon layer and carbon nanotube encapsuled Ni nanoparticles were prepared on α-Al2O3 support powder by rotary CVD using nickelocene as a precursor. The effect of deposition temperature (Tdep) on microstructure and compositions was investigated. The Ni content increased with increasing Tdep at 413–813 K. The highest Ni content was 2.1 mass% at 813 K. The carbon layer encapsuled Ni nanoparticlues was obtained at 613 K. Carbon nanotube encapsuled Ni nanoparticles was obtained at 893 K.