粉体および粉末冶金
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
テクニカルレポート
首里城破損瓦粉末を用いた放電プラズマ焼結
神田 康行
著者情報
ジャーナル オープンアクセス

2023 年 70 巻 3 号 p. 145-152

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This report investigated the spark plasma sintering (SPS) of Shuri castle breakage roof tile powder for the effective utilization of the Shuri castle breakage roof tiles. First, we examined the fundamental characteristics of Shuri castle breakage roof tiles. The chemical composition of broken roof tiles mainly comprises SiO2. Scanning electron microscopy analysis revealed the dispersion of quartz lumps in the inner structure. Additionally, the density of the broken roof tile was 2.43 g/cm3, and the open porosity was 17.9%, the Vickers hardness (HV) was 87.5 at the matrix side and 1200 at the quartz lump, and the flexural strength was 15.7 MPa. Meanwhile, the fundamental characteristics of the SPS compact formed using breakage roof tile powder comprised a density of 2.68 g/cm3, an open porosity of approximately 0%, an HV of 259, a flexural strength of 105 MPa, and a flexural modulus of 83.1 GPa at a sintering temperature of 1323 K. The formation of magnetite was confirmed via X-ray diffraction patterns of the sintered products; however, the crystalline phases were almost identical to those of the broken roof tile powders.

著者関連情報
© 2023 一般社団法人粉体粉末冶金協会

本論文はCC BY-NC-NDライセンスによって許諾されています.ライセンスの内容を知りたい方は,https://creativecommons.org/licenses/by-nc-nd/4.0/deed.jaでご確認ください.
https://creativecommons.org/licenses/by-nc-nd/4.0/deed.ja
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