Journal of the Japan Society of Powder and Powder Metallurgy
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
Quantitative Analysis of Tetragonal Phase in Mg-PSZ by X-ray Diffraction
Nobujiro TsuchiyaKazuhiko TsuchiyaMasahide FukudaKazuo Miyatani
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JOURNAL OPEN ACCESS

1995 Volume 42 Issue 9 Pages 1059-1062

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Abstract
A quantitative analysis of the tetragonal phase in Mg-PSZ by a standard X-ray powder diffraction method was carried out using the diffraction intensities with the Miller indices (311). The volume fraction of the tetragonal phase is shown to be given by
Vt=2.92/(1+0.991 X), where X={It(311)+Ic(311)}/It(113) which involves the diffraction intensities It and Ic of the corresponding tetragonal and cubic phases. The standard error of this method was estimated to be 4.5%. The present result is applicable to evaluate the tetragonal phase and the cubic phase in Mg-PSZ which contains the monoclinic phase less than 37%.
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© Japan Society of Powder and Powder Metallurgy

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