粉体および粉末冶金
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
Y-PSZの泥しょう鋳込成形と焼結(第1報)
泥しょう調製条件の検討
佐野 三郎小泉 憲一伴野 巧芝崎 靖雄小田 喜一
著者情報
ジャーナル オープンアクセス

1997 年 44 巻 9 号 p. 876-880

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抄録
This study is concerned with the fabrication of engineering ceramics parts with complicated shape by using slip casting process. Preparation conditions of slurries for 3 kinds yttria partially stabilized zirconia (Y-PSZ) powders were examined by the measurement of zeta-potential and viscosity. As the powder characteristics, the isoelectric points of Y-PSZ powders were determined from zeta-potential measurement to be pH7.9 and 9.0 for powders produced by hydrolysis and pH5.3 for a powder produced by neutralization coprecipitation. Well-dispersed slurries were found for Y-PSZ powders by adding organic polymer deflocculant (polycarboxilic ammonium) to the zeta-potential of the powder becoming enough high at the negative side. When the adding amount of deflocculant was shorted and the zeta-potential was around OmV, the viscosity of the slurry becoming very high and can't use for slip casting. In a case of a Y-PSZ powder produced by hydrolysis, low viscosity slurry can be prepared without adding deflocculant since the zeta-potential is high enough at the positive side.
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© 社団法人粉体粉末冶金協会

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