Journal of Japan Oil Chemists' Society
Online ISSN : 1884-2003
ISSN-L : 0513-398X
Determination of Solid Fat and Water Content of Margarine by High Resolution NMR
Teruo SUZUKIOsamu KAMOHiroshi TOYAMAKageo YOSHIDATakenori MARUYAMAIsao NIIYA
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1970 Volume 19 Issue 11 Pages 1019-1024

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Abstract
Authors attempted analysis for simultaneous determination of solid fat and water contained in margarine using NMR signal intensity method. The sample used were; different types of butters and margarines, blends of hardened beef tallow and corn-oil, with various amounts of water added to.
The solid fat content from high resolution NMR and the solid fat index (S.F.I.) value from dilatometry tended similar in the lower level, less than 25 of the S.F.I. value, but the difference between the both methods became 20% or more in the higher level, more than 40 of the S.F.I. value.
From the result of the quantitative analysis, the lowest detectable concentration of water was 3.4%. The accuracy of the area intensity method was found to be ±2% within the temperature range, 0° to 45°C.
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