Journal of Japan Oil Chemists' Society
Online ISSN : 1884-2003
ISSN-L : 0513-398X
Preparation of Lavandulyl Methyl Ether from Isoprene
Toru SATOHideo KISEManabu SENOTeruzo ASAHARA
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1975 Volume 24 Issue 4 Pages 265-267

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Abstract
Lavandulyl methyl ether was prepared by the following reactions : The addition of chloromethyl methyl ether to prenyl chloride in the presence of stannic chloride afforded 1, 3-dichloro-2-methoxymethyl-3-methylbutane, which was then treated in DMF to give the dehydrochlorination product, 2-methyl-3-methoxymethyl-4-chlorobutene-1. The Grignard reaction of the butene derivative with methallyl chloride gave lavandulyl methyl ether. The total yield of lavandulyl methyl ether was 3540% based on isoprene.
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