Journal of Surface Analysis
Online ISSN : 1347-8400
Print ISSN : 1341-1756
ISSN-L : 1341-1756
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Development of Ultra High Vacuum Transmission Electron Microscope for In Situ Observation of Silicides And Island Formation on Silicon Surface at High Temperatures by Reflection And Transmission Electron Microscope
J. KatoY. HigashiT. NagatomiY. Takai
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2002 Volume 9 Issue 2 Pages 150-159

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Abstract
An ultra high vacuum transmission electron microscope (UHV-TEM) has been successfully developed for in situ observation of the islands and silicides formation on silicon surface at high temperatures by reflection electron microscope (REM) and TEM. The cleaning process of the contaminated Si(100) surface by heating to 1150°C was successfully observed by REM. The thinning process of the Si(100) specimen by heating to 900°C with the oxygen exposure is dynamically observed by TEM. The observation of the surface steps on Si(100) with TEM is also carried out with considerable success. The present results lead us to the confirmation that the developed UHV-TEM can be applied to the study of the islands and silicides formation by in situ REM and TEM observation.
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© 2002 by The Surface Analysis Society of Japan
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