Journal of Surface Analysis
Online ISSN : 1347-8400
Print ISSN : 1341-1756
ISSN-L : 1341-1756
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Development of Evaluation Method of Sample Damage of Organic Material Caused by X-rays Irradiation on XPS. Results of Round Robin Test
S. TanumaA. AsoA. KoizumiM. SuzukiH. TohmaS. HashimotoK. Miura
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2002 Volume 9 Issue 4 Pages 501-509

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Abstract
We have carried out a round robin test for the evaluation of sample damage of polyvinyl chloride (PVC) and nitrocellulose and cellulose acetate (NC-CA) due to monochromatic X-ray irradiation, and obtained the following results. It is possible to evaluate the sample surface damage from the degradation rate constants of PVC and NC-CA sample if we use the special holder developed in this research. This hoder has a hole on substrate to prevent the diffusion of the heat and also has a thin metal plate cover to keep the sample surface flat. The resulting ratio of the degradation rate constant of PVA to that of NC-CA is a universal constant (0.174 ±0.015), which is independent from used XPS instrument. Then, PVC and NC-CA will be good specimens for the indicator of X-ray source flux
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© 2002 by The Surface Analysis Society of Japan
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