Journal of Advanced Science
Online ISSN : 1881-3917
Print ISSN : 0915-5651
ISSN-L : 0915-5651
Letter
Evaluation of MgB2 bulk structure prepared by hot-pressing method
Tsuneaki OBARA Hiroshi OHUCHIYutaka YAMADA
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2014 Volume 26 Issue 3+4 Pages 17-19

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Abstract
MgB2 bulks have been prepared by hot pressing method in order to fabricate high density MgB2 structure. Mixed Mg and B powder were enclosed in stainless steel mold. The bulk samples were treated at 850°C for 3 h under 30-300 MPa in Ar gas atmosphere. The hot pressed sample size is 20 mm in diameter and 5.6~10 mm in thickness. The XRD patterns of the bulks show that MgB2 phase is synthesized and dominant with small amount of MgO in the whole range of 0~300 MPa. The density of the bulks increased with increasing hot pressing pressure, and reached a peak of 2.34 g/cm3 at 200 MPa which corresponded to the relative density of 90 %.
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