Netsu Sokutei
Online ISSN : 1884-1899
Print ISSN : 0386-2615
ISSN-L : 0386-2615
Nanocalorimetry
Yoshitsugu Nakagawa
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2000 Volume 27 Issue 1 Pages 30-38

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Abstract
A new type of calorimetry which uses a micromechanical probe as a “bimetallic” temperature sensor is reviewed. The calorimetry has a theoretical heat detection limit of the order of 20fJ and a time resolution of 0.5ms. In the investigation of rotator phase transitions of n-alkanes, we obtained a heat sensitivity of 0.5nJ for a sample mass of 7pg with a time resolution of 0.5ms. Methods for precise quantification of the transition enthalpies are discussed.
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© Japan Society of Calorimetry and Thermal Analysis
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