The Proceedings of the Thermal Engineering Conference
Online ISSN : 2424-290X
2006
Session ID : A114
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A114 Screening of metastable C_<60> crystals using a microfluidic device
Kyosuke ShinoharaTakeshi FukuiHiroaki AbeNaoto SekimuraKoji Okamoto
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CONFERENCE PROCEEDINGS FREE ACCESS

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Abstract
We have synthesized C_<60> crystals using a simple liquid/liquid interfacial precipitation method in a mcrofluidic device. By controlling space, time, temperature, concentration, various C_<60> crystal morphologies were obtained including multiwalled tubes, open-ended hollow columns, dendrites, prisms, and needles. The C_<60> crystal morphologies were categorized mainly by temperature, and similar to the morphologies of snow crystals. This simple method yields complex geometries of C_<60> crystals quickly, and could be applied to all materials synthesis techniques that use liquid/liquid interfacial precipitation such as carbon crystals, protein crystals, clathrate hydrate crystals, and minerals.
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© 2006 The Japan Society of Mechanical Engineers
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