材料
Online ISSN : 1880-7488
Print ISSN : 0514-5163
ISSN-L : 0514-5163
電子デバイス用薄膜のヤング率測定用精密3点曲げ試験装置の開発と測定例
橋本 清司坂根 政男大南 正瑛吉田 敏博
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1994 年 43 巻 489 号 p. 703-709

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This paper describes the precision three-points bending machine developed for measuring Young's modulus of thin films used for electronic devices. The developed machine has 0.05μm displacement and 9.8×10-6N load resolution. The Young's modulus of 200μm glass plate in thickness measured by the machine agreed with that of the published value within 3% difference, which shows that the machine has a sufficient performance and reproducibility of the data. The Young's moduli of sputtered Co-Ta-Zr amorphous thin films, of which thickness were ranged from 1μm to 10μm, were measured. The Young's moduli of the thin films thicker than 4.5μm showed a constant value of 150GPa, but those smaller than 4.5μm in thickness increased with decreasing film thickness. The Young's modulus of 1μm in thickness showed a value of 250GPa which is about 70% larger than that of 10μm in thickness. The Young's moduli measured for the films more than 4.5μm in thickness well agreed with the bulk Young's modulus of amorphous Co alloy.
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