材料
Online ISSN : 1880-7488
Print ISSN : 0514-5163
ISSN-L : 0514-5163
シリコン単結晶のX線応力測定
鈴木 裕士秋田 貢一三沢 啓志
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2000 年 49 巻 5 号 p. 534-540

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In the X-ray stress measurement of single crystal, crystal oscillation operation is required in order to obtain perfect diffraction profile. Accurate diffraction profiles can be measured by using the χψ-oscillation method proposed in this study. Using this oscillation method, the elasticity applied stress measurement of the silicon single crystal used as a material of semiconductor device was carried out. Lattice strain was obtained from peak shift of diffraction profile. Stress was calculated by using lattice strain of three different diffraction planes. As a result, the measured stress agree well with the applied stress evaluated from a strain gage. Therefore, the possibility of elastically applied stress measurement of the single crystal by the χψ-oscillation method was confirmed. Also, the relationship between setting error of the test piece and stress error was theoretically examined. It was confirmed that the effect of misalignment on X-ray stress measurement of single crystal materials is much larger than in the case of polycrystalline materials. In this study, a microscope was used to set the specimen.
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