真空
Online ISSN : 1880-9413
Print ISSN : 0559-8516
ISSN-L : 0559-8516
α-オレフィンとジフェニルの反応による拡散ポンプ油の合成
渡辺 昭次中根 敏章
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ジャーナル フリー

1969 年 12 巻 1 号 p. 29-31

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A mixture of diphenyl and a-olefin (C11-C15 mixture) in the presence of anhydrous aluminium chloride was heated at 150°C to give a pale yellow oil boiling at 180-200°C/10-4 Torr. This oil has an excellent properties for a diffusion pump oil, for instance, the ultimate pressure was measured by Hickman type glass diffusion pump, and we certified the order of 10-7 Torr, as showed in Table 4, and thermal decomposition rate was also measured as shown in Table 5. which we realized this rate is comparably low.
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