Journal of the Vacuum Society of Japan
Online ISSN : 1882-4749
Print ISSN : 1882-2398
ISSN-L : 1882-2398
Review
Present Stage of Sub-nanometer Analysis by Aberration-corrected Scanning Transmission Electron Microscopy
Naohiko KAWASAKI
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2013 Volume 56 Issue 9 Pages 360-364

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Abstract
  Scanning transmission electron microscopy (STEM) is a powerful tool for not only imaging but also elemental composition and chemical bonding analysis by energy dispersive X-ray spectroscopy (EDX) and electron energy-loss spectroscopy (EELS) with nanometer spatial resolutions. The technique of spherical aberration correction has recently been developed, and angstrom spatial resolutions have been achieved for EDX and EELS measurement as well as imaging.
  I also introduce other recent trends in STEM related techniques. Low acceleration voltage has often been adopted in order to reduce electron radiation damage. Recent monochrometer has achieved 0.2 eV energy resolution for EELS measurement, which enables us to analyze chemical bonding in more detail. A new type of silicon drift detector (SDD) improves the sensitivity of EDX 10 times higher than conventional detectors. These recent technologies are not independently implemented but combined in an ultimate system which can promote diverse applications of STEM.
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© 2013 The Vacuum Society of Japan
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