KAGAKU KOGAKU RONBUNSHU
Online ISSN : 1349-9203
Print ISSN : 0386-216X
ISSN-L : 0386-216X
Particle Technology and Fluidizations
Gas-Phase Synthesis of Fine Silica Particles from Tetramethoxysilane
Toshinori KOJIMATsuyoshi UCHIYAMAShigeru KATOUHiromitsu SHIBUYAShigeyuki UEMIYA
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2004 Volume 30 Issue 3 Pages 306-310

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Abstract
Highly efficient silica products are widely used in the semiconductor industries. Generally this type of silica is produced by a liquid-phase method, which entails various limitations. In this communication, we report a method for manufacturing silica in the gaseous phase by hydrolyzing alkoxysilane. The operation conditions of the gaseous-phase reactions during the synthesis of silica were optimized. The influences of temperature, gas flow rate and concentrations on the reaction kinetics (particle production rate) were also investigated. Products were characterized by SEM. Results indicated that the silica particle diameters could be controlled by changing reaction conditions.
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© 2004 by THE SOCIETY OF CHEMICAL ENGINEERS, JAPAN
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