MATERIALS TRANSACTIONS
Online ISSN : 1347-5320
Print ISSN : 1345-9678
ISSN-L : 1345-9678
Microstructure of Materials
In Situ Scanning Electron Microscopy Observation of Sintering Process of Aluminum Alloy
Naoki OyaTatsuya SatoDaichi Yamaguchi
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2023 年 64 巻 8 号 p. 1946-1951

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Binder jetting (BJT) holds enormous promise as an additive manufacturing technique due to its high throughput and low-cost equipment. The ability to fabricate geometrically complex parts from aluminum alloy via BJT would have a significant impact on the development of high-performance machine components and heat-dissipation devices. However, processing printed objects by sintering of aluminum alloy is difficult due to the surface oxide layer that covers the powder particles, which prevents the final parts from reaching a sufficiently high density. In order to investigate the sintering mechanism for controlling the quality of sintered parts, we directly observed the sintering behavior of pure Al and Al–10%Si–0.4%Mg (mass%) alloy using an in situ scanning electron microscopy system equipped with a heating stage. It is found that the surface roughness of the powder particles is reduced above their melting or solidus temperature. Subsequently, the liquid ruptures the oxide layer and forms necks between the particles.

 

This Paper was Originally Published in Japanese in J. Jpn. Soc. Powder Powder Metallurgy 68 (2021) 311–316.

Fig. 6 In situ SEM images of Al–10%Si–0.4%Mg powder at 800×: (a) before heating, (b) at 564°C (liquid fraction: 0 mass%), (c) at 569°C (liquid fraction: 7 mass%), (d) at 574°C (liquid fraction: 49 mass%), (e) at 594°C (liquid fraction: 100 mass%). (f) Temperature dependence of liquid mass fraction showing points (a)–(e). Fullsize Image
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© 2023 Japan Society of Powder and Powder Metallurgy
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