We present a method to treat suspension contaminated with trichloroethylene (TCE). We aimed to remove TCE and precipitate the fine particles in the suspension using ultrasound irradiation. The solution was prepared from ion-change water and TCE. The suspension was prepared from the solution and green tuff. TCE solution (500ppm) was completely decomposed by 2h sonication in argon atmosphere. And the complete decomposition of TCE in suspension (500ppm) was also confirmed at the same condition. The decomposition rate of TCE in solution and suspension were almost same. Isoelectric zone of green tuff suspension was 1.4-3.8 in pH. The degradation of TCE acidified the solution and brought the pH level of the suspension to the isoelectric zone. Thus, it is feasible to remove TCE and precipitate fine particles in the suspension using ultrasound irradiation.