日本セラミックス協会 年会・秋季シンポジウム 講演予稿集
16th Fall Meeting of The Ceramic Society of Japan & The 5th International Meeting of Pacific Rim Ceramic Societies(PacRim5)
セッションID: 05-P-04
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Effect of Atmospheric Pressure during Sintering on Mechanical Properties and Microstructure of Hot-Pressed SiC Containing Y2O3-SiO2 Additives
*Hirofumi INOUEKeiichi KATAYAMAToyohiko YANOMasamitsu IAMI
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Silicon carbide (SiC) powders with total 11 mass% of Y2O3 and SiO2 additives were sintered by hot-pressing at 1950oC for 1h under a pressure of 40 MPa in Ar flow or 1MPa Ar atmosphere. Bending strength, microstructure, oxygen content of the sintered specimens were evaluated. The sintered bodies achieved nearly full density in the wide range of additive composition in both cases. The dispersion of bending strength was remarkable in the case of Ar flow sintering.SEM micrographs revealed the difference in microstructure between inside and outside of sintered bodies. Oxygen content was also different between inside and outside of sintered bodies. These results suggest that volatilization of additives. After sintering under 1MPa atmospheric pressure, microstructural difference between outside and inside bodies was greatly reduced, and bending strength of sintered bodies showed constant values.
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© The Ceramic Society of Japan 2003
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