日本セラミックス協会 年会・秋季シンポジウム 講演予稿集
16th Fall Meeting of The Ceramic Society of Japan & The 5th International Meeting of Pacific Rim Ceramic Societies(PacRim5)
セッションID: 08-P-02
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Quick Fabrication of Highly Oriented Bi-2223 Superconducting Ceramics Using Plate-Like Seed Crystals
*Hidenobu ITOHKoji TAKEDAMasami KISHIJunichi TAKAHASHI
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We have successfully prepared plate-like fine powder of 2223 phase superconducting oxide with preferential 002 faces by grinding in dehydrated pure ethanol. In the present study, we attempted a quick fabrication of highly oriented (Bi,Pb)2Sr2Ca2Cu3Ox superconductor using the plate-like seed crystals. It was found that the addition of the seed crystals to commercial precursor (Dowa kogyo Co. Ltd.) brought about a considerable reduction in fabrication time. Almost all single phase (2223) sintered superconducting oxide was obtained by heating of the precursor mixed with 30 wt% seed crystals for 4 hr at 870 C. Furthermore, the grains of the sintered disk were highly oriented.
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© The Ceramic Society of Japan 2003
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