Preprints of Annual Meeting of The Ceramic Society of Japan
Preprints of Fall Meeting of The Ceramic Society of Japan
16th Fall Meeting of The Ceramic Society of Japan & The 5th International Meeting of Pacific Rim Ceramic Societies(PacRim5)
Session ID : 14-P-37
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Measurement of Lattice Defect and Local Strain in Polished Sapphire by TEM
*Tomohiro SAITOHiroshi KAWAMOTOTakahisa YAMAMOTOYuichi IKUHARA
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Abstract
Lattice defect and local strain, which were introduced by systematically machining the basal plane of sapphire, ware characterized by cross-sectional transmission electron microscopy (XTEM) and convergent beam electron diffraction (CBED) It was found that dislocations and strain were introduced from the surfaces for all specimens examined in this study. Depths of the introduced dislocations were measured by weak beam dark field (WBDF) method, and residual strain in the vicinity of the surfaces were precisely measured by CBED method using the probe size less than 10nm. Maximum penetration depths of the dislocations in the specimens ground with #500 diamond wheel, polished with 4~8μm and under 1μm diamond slurry were 1.7μm, 700nm and 250nm, respectively. Residual local strain was found to remain at the depths of 1.0μm, 1.2μm and 300nm for the specimens ground with #500 diamond, polished with 4~8μm and under 1μm diamond slurry, respectively.
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© The Ceramic Society of Japan 2003
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