Preprints of Annual Meeting of The Ceramic Society of Japan
Preprints of Fall Meeting of The Ceramic Society of Japan
21st Fall Meeting of The Ceramic Society of Japan
Session ID : 2J08
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Examination of spark-plasma-sintering condition for attaining transparent spinel
*Koji MoritaHidehiro YoshidaByung-Nam KimKeijiro Hiraga
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Abstract
Optimum spark-plasma-sintering processing was examined in order to fabricate transparent spinel polycrystal. For a low heating rate of 10C/min, in-line transmission T of spinel polycrystal depends strongly on sintering temperature, particular in visible-wavelength ranges. For a infrared-wavelength of 2000nm, T(2000) attains 60-70% irrespective of temperature. For a visible-wavelength of 550nm, however, T(550) varies from 2 to 50% depending on sintering temperature; T(550) shows a peak value of about 50% at around 1300C. The temperature dependent in-line transmission can be ascribed to the change in microstructure such as grain size, resultant residual porosity and the precipitation of MgO phase.
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© The Ceramic Society of Japan 2008
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