1972 年 58 巻 10 号 p. 1424-1437
An investigation was made of the effect of Nb on the refinement of ferrite grain size in hot-rolled low-carbon steels.
Experiments of hot-rolling by 2-passes were performed using 11 vacuum-melted steels with various C, N, Nb, and V contents. The main results are as follows:
(1) In Si-Mn steels not containing such special elements as Nb, the coarse grains of austenite at soaking temperature are recrystallized into fine grains during hot-rolling. The relation between the austenite grain size just above Ar3 and the transformed ferrite grain size is similar whether the process contains hot-rolling or not.
(2) In the steels containing comparatively large amounts of Nb or, when hot-rolled at relatively low temperatures, in the steels containing small amounts of Nb, the austenite can not recrystallize during cooling from finish-rolling temperature to Ar3 and transforms to ferrite of finer grains. Ferrite grains nucleate around the deformation bands in unrecrystallized austenite grains as well as at the austenite grain boundaries.
Mixed grain and/or upper-bainitic structures sometimes appear after transformation.
(3) The retardation of recrystallization of austenite during hot-rolling process in Nb-containing steels is due to NbC (N) which has been in solution at soaking temperature and finely precipitates during hotrolling. Hot-rolling accelerates such precipitation. Therefore, when finish-rolled at a higher temperature, the austenite of steels containing small amounts of C, N, and Nb recrystallizes completely.
(4) When the austenite recrystallizes completely during cooling to a temperature just above Ar3, the presence of precipitates, as NbC (N) or VN, can contribute to the refinement of ferrite grain size, probably by retarding the growth of ferrite grains.