鉄と鋼
Online ISSN : 1883-2954
Print ISSN : 0021-1575
ISSN-L : 0021-1575
水素気流中加熱抽出法による鋼中非金属元素状態分析装置の開発
大坪 孝至宮坂 明博安田 浩
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1983 年 69 巻 1 号 p. 153-162

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A new technical method has been developed on the analytical system which can provide us with the information about the phase of nonmetallic elements, such as carbon, sulfur and nitrogen, in steel.
When a finely-milled steel sample is isochronally heated in a hydrogen stream, nonmetallic elements react with hydrogen forming hydride-gases. The hydrides are at real-time analysed by a mass-spectrometer in relation to the heating temperature. From the temperature and the amount of gas detected, the phase of nonmetallic elements in steel is analysed.

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