1991 年 77 巻 12 号 p. 2163-2170
A technique for particle size distribution measurement of Al2O3 inclusion in ultra low oxygen steel by combination of ultrasonic classification method and centrifugal sedimentation photo-extinction method has been established.
The procedure is as follows.
(1) The Al2O3 inclusion extracted from steel by acid decomposition is classified at over and under 5μm with ultrasonic filtration.
(2)The Al2O3 inclusion over 5μm is weighed.
(3) The particle size distribution of Al2O3 inclusion under 5μm is measured automatically with centrifugal sedimentation photo-extinction method.
(4)The particle size distribution of Al2O3 in steel can be obtained by using from (1) to (3).
This technique makes it possible to measure particle size distribution of Al2O3 to sub-micron order, and gives instructive information about coalescence and/or floating behavior of Al203 inclusion during refining prosess.