Crystal Structure of 4-Bromo benzoylmethylenediphenyldiphenylphosphinomethylphosphorane

Seyyed Javad SABOUNCHEI; Sepideh SAMIEE; David MORALES-MORALES; Simon HERNANDEZ-ORTEGA

doi:10.2116/xraystruct.27.3

Part 1

Crystal Structure of 4-Bromo benzoylmethylenediphenyldiphenylphosphinomethylphosphorane

Seyyed Javad SABOUNCHEI, Sepideh SAMIEE, David MORALES-MORALES, Simon HERNANDEZ-ORTEGA

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Supplementary material

2011 Volume 27 Pages 3-4

DOI https://doi.org/10.2116/xraystruct.27.3

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Abstract

The crystal structure of 4-bromo benzoylmethylenediphenyldiphenylphosphinomethylphosphorane was determined by X-ray crystallography. The compound crystallized in a monoclinic system and was characterized thus: P2₁/c, a = 13.3489(16)Å, b = 18.933(2)Å, c = 11.3211(14)Å, β = 101.735(2)°, Z = 4, V = 2801.4(6)Å³. The crystal was solved by direct methods and refined by full-matrix least-squares on F² to final values of R₁ = 0.0379 and wR₂ = 0.0682.

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