X-ray Structure Analysis Online
Online ISSN : 1883-3578
ISSN-L : 1883-3578
Part 1
Synthesis and Crystal Structure of a Nickel(II) Complex with Bis(2-methoxyethyl)amine
Ryo YAMAGUCHIMoriya TASAKIEiji ASATOHiroshi SAKIYAMA
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2011 Volume 27 Pages 5-6

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Abstract
The nickel(II) complex [Ni(bmoen)2(DMF)](BPh4)2·DMF [bmoen = bis(2-methoxyethyl)amine, DMF = N,N-dimethylformamide], was synthesized and characterized by single-crystal X-ray analysis. The compound crystallizes in the monoclinic spaces group P21/n and Z = 4 with cell parameters a = 11.690(2)Å, b = 29.013(5)Å, c = 17.856(3)Å, β = 90.345(2)°, V = 6056(2)Å3. One of the bmoen ligands works as a tridentate ligand in a fac (facial) form, and the other bmoen ligand works as a bidentate ligand.
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© 2011 by The Japan Society for Analytical Chemistry
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