Abstract
Bis[pentafluorophenyl[24]dithahexaphyrin(1.0.0.1.0.0)] 1, molecular formula C100H74F20N8S4, was isolated in this study. The crystal structure of the title compound was determined by single-crystal X-ray diffraction at 150(2)K, and was assigned to the monoclinic space group P21/c with a = 17.755(4)Å, b = 21.580(4)Å, c = 25.600(5)Å, β = 102.312(3)°, V = 9583(3)Å3, Dx = 1.314 g/cm3, and Z = 4. From 16887 independent reflections, R1 [I > 2σ(I)] and wR2 were determined to be 0.0716 and 01467, respectively. These values were calculated for all reflection data.
