X-ray Structure Analysis Online
Online ISSN : 1883-3578
ISSN-L : 1883-3578
Part 5
Crystal Structure of N,N′-Bis(4-hexyloxybenzoyl)piperazine
Kanji KUBOEmi YAMAMOTOTaisuke MATSUMOTOAkira MORI
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Supplementary material

2016 Volume 32 Pages 19-20

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Abstract

The structure of N,N′-bis(4-hexyloxybenzoyl)piperazine was determined by X-ray crystallography. It crystallizes in the space group P21/c (#14) with cell parameters a = 27.234(7)Å, b = 7.496(2)Å, c = 6.820(2)Å, β = 93.80(2)°, Z = 2, and V = 1389.3(6)Å3. The molecule sits on a center of symmetry, such that the two benzoyl groups are in an anti conformation with respect to one another across the piperazine ring. Intermolecular C–H···O and C–H···π interactions were observed in the crystal lattice.

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© 2016 by The Japan Society for Analytical Chemistry
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