Part 9
Crystal Structure of 6-Aza-3,9-dithiaundecane Hydrochloride
2019 年 35 巻 p. 55-56
詳細
2019 年 35 巻 p. 55-56
The crystal structure of the title compound, 6-aza-3,9-dithiaundecane hydrochloride (N-H-ATU·HCl), was determined by X-ray crystallography. The hydrogen-bonding networks in the crystal extend along with the b and c axes to form a 2D-triple-sheet, in which the Cl− ions put between two (N-H2-ATU)+ sheets. The compound was crystallized in an orthorhombic system as: Pccn, a = 25.0091(4), b = 5.39364(10), c = 9.37759(19)Å, Z = 4, V = 1264.94(4)Å3. The R1 and wR2 values were 0.0341 and 0.0880, respectively, for 1162 reflections.
