Journal of Synthetic Organic Chemistry, Japan
Online ISSN : 1883-6526
Print ISSN : 0037-9980
ISSN-L : 0037-9980
The Apparatus of Thermal Analysis
Studies of DTA and EGA for Organic Synthesis under High Gaseous Pressure. (Part 1)
Koki OTA
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1971 Volume 29 Issue 8 Pages 796-798

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Abstract

An apparatus for simultaneous differencial thermal and evolved gas analysis under high pressure, useful in the field of organic synthesis under various gaseous pressure, was developed.
It consists principally of a couple of particular small steel autoclaves, glass sample containers and thermal and pressure detectors.
The behavior of potassium phenoxide and mono potassium p-hydroxy benzoate under carbon dioxide pressure was studied by using the apparatus.

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© The Society of Syhthetic Organic Chemistry, Japan
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