Purpose: To evaluate the effects of different surface treatments on the tensile bond strengths of a resin cement to zirconia ceramics.
Materials and Methods: Zirconia discs (Lava) were fabricated and the surfaces of the specimens were ground with #600-grit SiC paper. Then the specimens were divided into four groups according to the surface treatment: (1) no pretreatment (control); (2) air-abrasion with 110 µm Al2O3; (3) laboratory tribochemical silica coating (Rocatec) with 110 µm Al2O3 and 30 µm silica modified Al2O3; (4) coating the surface (INT coating) with silica-based porcelain (Vintage ZR). Each group was subsequently divided into two subgroups assigned to be silanated using a ceramic primer (RelyX Ceramic Primer) or not. The bonding procedure was then performed using a dual-cure resin cement (RelyX ARC). After 24 h storage in water, the specimens were thermocycled (5-55˚C, 5,000 cycles). The bonding performance was evaluated by the tensile bond strength test. Statistical analyses were performed at the level of p=0.05.
Results: The control groups showed the lowest bond strengths. The silanated groups showed significantly higher bond strengths than the non-silanated groups for each surface condition (p>0.05). The highest bond strength (27.2±6.2 MPa) was provided by the INT coating group with silanization. However, no significant difference was obtained between the INT coating and Rocatec groups after silanization (p>0.05).
Conclusion: With silanization, the INT and tribochemical silica coatings were the most effective in improving the bond strengths of the resin cement to zirconia ceramics.
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