Journal of The Adhesion Society of Japan
Online ISSN : 2187-4816
Print ISSN : 0916-4812
ISSN-L : 0916-4812
Technical Report
Microencapsulation of Aqueous Solution of Hardening Agent for Adhesive Based on Starch -Effects of Preparation Conditions on Microencapsulation-
Ken HAGANOKiyomi FUCHIGAMIYoshinari TAGUCHIMasato TANAKA
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2007 Volume 43 Issue 1 Pages 13-19

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Abstract
The sodium hydroxide aqueous solution as a hardening agent for the adhesive made of starch was microencapsulated with polymer melted at about 90℃. Microcapsules were prepared by the suspension polymerization method using styrene and ethyl hexyl aclylate monomers. In the experiment, the concentration of oil soluble surfactant, the prebulkpolymerization time and the impeller speed for preparing (W/0)/W dispersion were changed stepwise. It was investigated how these operating conditions affected the content of core material, the mean diameter and the inner structure of microcapsules. The sodium hydroxide aqueous solution could be microencapsulated under all the experimental conditions adopted here and released at about 90℃.The content of core material was decreased with the impeller speed, increased with the prebulkpolymerization time and became maximum at the concentration of surfactant of 1.0wt%.
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© 2007 The Adhesion Society of Japan
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