Analytical Sciences
Online ISSN : 1348-2246
Print ISSN : 0910-6340
ISSN-L : 0910-6340
Notes
Determination of Triazine Pesticides and Related Compounds in Environmental Water by Liquid Chromatography-Mass Spectrometry
Akiko TANABEKuniaki KAWATA
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ジャーナル フリー

2004 年 20 巻 1 号 p. 227-230

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A method for the determination of 5 triazine herbicides and 12 degradation products in environmental water samples using liquid chromatography-electrospray ionization mass spectrometry (LC/ESI/MS) has been developed. The pesticides in water were extracted with two types of solid phase: a styrene-divinylbenzene copolymer and a graphitized carbon black. Desorption solvents for the extracted compounds were acetone for the styrene-divinylbenzene copolymer and methanol for the graphitized carbon black. Overall recoveries from ground water and river water ranged from 73% to 111%. The limits of detection (LODs) were 0.2 to 28 ng l-1. This method was applied to several ground water samples.
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© 2004 by The Japan Society for Analytical Chemistry
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