Analytical Sciences
Online ISSN : 1348-2246
Print ISSN : 0910-6340
ISSN-L : 0910-6340
Notes
A Clean-up Method by Photocatalysis for HPLC Analysis of Iprodione in Dry Basil
Osamu MAEDAChie OIKAWANobuo SHIOMIAkira TORIBAKazuichi HAYAKAWA
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2008 Volume 24 Issue 8 Pages 1053-1055

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Abstract
Titanium dioxide was used as a photocatalyst to decompose interfering substances for a quantitative analysis of a fungicide (iprodione) in dry basil by HPLC. A quartz vial containing basil extract and titanium dioxide was irradiated with black light. The interfering substances were almost completely decomposed by 180 min of irradiation, whereas 88.3% of iprodione remained. The recovery of iprodione was 102.6% by the proposed method in basil extracts. This may have been due to different decomposition rates of the analyte and interfering substances.
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© 2008 by The Japan Society for Analytical Chemistry
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