Analytical Sciences
Online ISSN : 1348-2246
Print ISSN : 0910-6340
ISSN-L : 0910-6340
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Development of Online Dilution System for Quantification of 90Sr Using Automatic Solid-phase Extraction Inductively Coupled Plasma Mass Spectrometry
Kayo YANAGISAWAMakoto MATSUEDAMakoto FURUKAWAYoshitaka TAKAGAI
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2020 Volume 36 Issue 9 Pages 1131-1135

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Abstract

In this paper, we propose an online dilution system for the rapid quantification of radioactive strontium-90 (90Sr) with inductively coupled plasma mass spectrometry coupled solid-phase extraction and O2 dynamic reaction (cascade ICP-MS). The proposed system automatically provides a higher dilution ratio, which is at most 3.3 ± 0.2-times the ratio obtained by the previous method, without increasing the analysis time (<15 min). A detection limit of 2.7 Bq/kg wet (0.54 pg/kg wet) was achieved. The recovery test results were consistent with two different spiked values.

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© 2020 by The Japan Society for Analytical Chemistry
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