Analytical Sciences
Online ISSN : 1348-2246
Print ISSN : 0910-6340
ISSN-L : 0910-6340
Development of Preconcentration by Continuous Sulfide Precipitation-Dissolution in ICP-AES
Young Min ChoYong-Nam Pak
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1997 年 13 巻 Supplement 号 p. 41-44

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The technique of on-line direct precipitation preconcentration by sulfide precipitation for As has been developed and applied to ICP-AES. For 1.0mL of sample, the enrichment factor is 4 with the sampling speed of 15/hr. However, the enrichment factor can be increased to more than 40times when the sampling volume is increased to 10mL with the samplig speed of 5/hr. Analysis of NIST reference material yielded a good result with the certified value.
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© The Japan Society for Analytical Chemistry
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