Analytical Sciences: X-ray Structure Analysis Online
Online ISSN : 1348-2238
ISSN-L : 1348-2238
Part 6
Crystal Structure of Tricyclohexyltin N,N′-Di-n-butyl-dithiocarbamate
Xueqing SONGRobert PIKEGeorge ENG
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2006 年 22 巻 p. x137-x138

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The title compound, [C27H51NS2Sn], crystallized in a monoclinic space group P21/n with the following cell parameters: a = 10.13770(10), b = 27.9513(4), c = 10.82300(10)Å, β = 106.6070(10)°, V = 2938.90(6)Å3, Z = 4, and Dx = 1.294 Mg/m3. The structure was refined to a final R value of 0.0232 for 5267 reflections [I > 2 σ(I)]. The structure can be best described as a distorted tetrahedron owing to the presence of a long intramolecular Sn…S interaction.
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© 2006 by The Japan Society for Analytical Chemistry
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