Analytical Sciences: X-ray Structure Analysis Online
Online ISSN : 1348-2238
ISSN-L : 1348-2238
Part 2
X-ray Investigation of Bicyclic α-Methylene-δ-valerolactones. VI. (4aS,7S,8aS)-7-Isopropenyl-4a-methyl-3-methyleneperhydro-chromen-2-one
Jakub WOJCIECHOWSKIHenryk KRAWCZYKMarcin SLIWINSKIWojciech M. WOLF
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ジャーナル フリー

2008 年 24 巻 p. x25-x26

詳細
抄録
Enantiomerically pure (4aS,7S,8aS)-7-isopropenyl-4a-methyl-3-methyleneperhydro-chromen-2-one, C14H20O2, crystallized in an orthorhombic system: cell constants a = 6.565(1), b = 10.880(2), c = 17.716(4)Å; V = 1265.5(4)Å3; space group P212121 Z = 4. The title compound adopts a semi-folded conformation in which the δ-valerolactone and cyclohexane rings are almost perpendicular to one another. Both oxygen atoms are not involved in nonbonding intramolecular contacts with the neighboring atoms.
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© 2008 by The Japan Society for Analytical Chemistry
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