Utilization of 13C-13C Coupling in Structural and Biosynthetic Studies Double Labeling Method

Haruo SETO; Tsutomu SATO; Hiroshi YONEHARA

doi:10.1271/bbb1961.39.1667

Agricultural and Biological Chemistry

Online ISSN : 1881-1280
Print ISSN : 0002-1369
ISSN-L : 0002-1369

Utilization of ¹³C-¹³C Coupling in Structural and Biosynthetic Studies Double Labeling Method

Haruo SETO, Tsutomu SATO, Hiroshi YONEHARA

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1975 Volume 39 Issue 8 Pages 1667-1672

DOI https://doi.org/10.1271/bbb1961.39.1667

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Abstract

A new method which utilizes ¹³C-¹³C coupling for structuual and biosynthetic studies on acetate-derived metabolites is describde. The ¹³C-NMR spectra of dihydrolatumcidins separately labeled with ¹³CH₃¹³CO₂Na and a 1:1 mixture of ¹³CH₃CO₂Na and CH₃¹³CO₂Na gave enough information to establish its structure.

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