繊維学会誌
Online ISSN : 1884-2259
Print ISSN : 0037-9875
多孔質アクリル繊維中に不規則に発達した孔の形態観察
川崎 史郎芦田 守釜口 知子島村 薫
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1993 年 49 巻 7 号 p. 389-392

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A new method for produsing replicas of pores in porous acrylic fibers has been developed for transmission electron microscopy. The method involved filling the pores with styrene followed by its polymerization. The resulting fibers impregnated with polystyrene were microtomed into sections of thickness of ca. 70nm, from which acrylic part was removed by extraction with dimethyl sulfoxide. This procedure resulted in pore replicas with minimum of artifacts. Application of this method to the wet spun acrylic fibers revealed morphology of the internal pore networks which were slightly oriented along the fiber axis.
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