1989 年 97 巻 1131 号 p. 1432-1434
A precursor for borosilicate fibers was prepared by a new method via polyborosiloxane (PBS) prepared by condensation polymerization of silicon tetraacetate (STA) with boron trialkoxide (BTA). A spinnable polymer was obtained from PBS by partial alkoxylation, subsequent hydrolysis, and aging for various time periods.