燃料協会誌
Online ISSN : 2185-226X
Print ISSN : 0369-3775
ISSN-L : 0369-3775
石炭中の炭酸塩の形の二酸化炭素の定量に関する研究第2報
圧力法の分析所内・所間精度と適用範囲
藤森 利美浦辺 太郎石川 馨似鳥 次郎桜井 康三遠藤 正
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1973 年 52 巻 5 号 p. 354-359

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The authors have studies in the first report on the pressometric and gravimetric methods for the determination of carbon dioxide in coals and concluded that the modified pressometric method (ISO/TC 27-490) was suitable for the specification in JIS.
It is necessary to specify a scope and tolerances when a method is accepted in JIS. The authors, therefore, have studied for this purpose, and concluded as follows:
1) The carbon dioxide evolved when low rank coals which belong to class III (Subbituminous) and IV (Lignitic) in ASTM D 388 “Classification of coals by rank” are treated with hydrochloric acid does not usually originate from carbonate minerals. These low rank coals, therefore, should be omitted from the scope of the JIS.
2) Tolerances calculated from the results of interlaboratory experiment are shown in the next table with that of other standards. The precisions of this method are consi-dered as fairly good figure in comparison with that of other standards.
The draft JIS M 8813-1972 has been prepared based on the above studies, and it will be published in the end of 1972.
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