Journal of Nutritional Science and Vitaminology
Online ISSN : 1881-7742
Print ISSN : 0301-4800
ISSN-L : 0301-4800
Separation and Partial Purification of Wax and Fatty Alcohol from Okinawan Sugar Cane Rind. Lipids
尚 弘子知念 功内原 京子
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1983 年 29 巻 3 号 p. 313-322

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A composition analysis of Okinawan sugar cane rind materials was conducted, and it was found that the main components were lipids, crude fiber and water indicating about 27%, 19.6% and 14.6%, respectively. The lipids were effectively extracted from rind materials by benzene. Wax (18%) and fatty alcohol (8%) were found to be the main components, totaling up to 96% of the lipids.
Separation and partial purification of wax and fatty alcohol were attempted by means of silica gel column chromatography, thin-layer chromatography (TLC), infrared (IR) absorption spectra and gas-liquid chromatography-mass spectrometry (GC-MS).
The major components of the wax were considered to be two compounds with the molecular weights of 408 (C-26) and 436 (C-28), and those of fatty alcohol were di-ol with molecular weights of 440 (C-29) and 468 (C31). Both wax and fatty alcohol were purified by rechromatography on a silica gel column and the samples obtained seemed to be satisfactory for use in experimental rats' diets.
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