Journal of Oleo Science
Online ISSN : 1347-3352
Print ISSN : 1345-8957
ISSN-L : 1345-8957
General Subjects
Difatty Acyl Urea from Corn Oil: Synthesis and Characterization
Emad A. Jaffar Al-MullaWan Md. Zin Wan YunusNor Azowa Bt IbrahimMohd Zaki A. Rahman
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JOURNAL FREE ACCESS

2010 Volume 59 Issue 3 Pages 157-160

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Abstract

In this study, difatty acyl urea has been successfully synthesized from corn oil using sodium ethoxide as a catalyst. Ethyl fatty ester and glycerol were produced as by-products. In this reaction, corn oil was refluxed with urea in ethanol. The highest conversion percentage (78%) was obtained when the process was carried out for 8 hours using urea to corn oil ratio of 5.6: 1.0 at 78°C. Both difatty acyl urea and ethyl fatty ester have been characterized using elemental analysis, Fourier transform infrared (FTIR) spectroscopy and 1H nuclear magnetic resonance (NMR) technique

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© 2010 by Japan Oil Chemists' Society
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