Abstract
We present a method of three-dimensional observation of internal defects in semiconductor crystals for blue lasers by use of two-photon process. We excite photoluminescence by using two-photon process. Since semiconductor materials have intrinsically high absorption in the short-wavelength region, the excitation light of photoluminescence is largely absorbed by the crystals. It is difficult to observe defects in deep regions. Two-photon excitation can overcome this limitation because near-infrared light is absorbed at only the focused point. The excitation light can penetrate into the deep retions of the crystal. We succeeded in observing defects in a ZnSe crystal 200 μm below the crystal surface.