MATERIALS TRANSACTIONS
Online ISSN : 1347-5320
Print ISSN : 1345-9678
ISSN-L : 1345-9678
Oxidation Resistance of Boiler Steels with Al2O3–Y2O3 Nano- and Micro-Composite Coatings Produced by Sol–Gel Process
Mingming YaoYedong HeWei ZhangWei Gao
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2005 Volume 46 Issue 9 Pages 2089-2092

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Abstract
Al2O3–Y2O3 nano- and micro-composite coatings have been deposited on boiler steel substrates using sol–gel composite coating technology. The processes include dipping samples in a sol–gel solution dispersed with fine ceramic powders, which is prepared by high-energy ball milling. Scanning electron microscopy (SEM) and XRD analyses show that the one-layer coating (i.e. dipping for one time) has a thickness of more than 2 μm. The coating is mainly composed of α-Al2O3 and γ-Al2O3, and is relatively dense without cracking after drying and sintering treatments. The oxidation tests performed in air at 600°C show that the coatings possess much improved resistance to high temperature oxidation and scale spallation. It is believed that the nano-structured composite particles and reactive elements are integrated into the coatings, which played an important role in improving their oxidation resistance.
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© 2005 The Japan Institute of Metals and Materials
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