MATERIALS TRANSACTIONS
Online ISSN : 1347-5320
Print ISSN : 1345-9678
ISSN-L : 1345-9678
Magnetic-Domain Structure Analysis of Nd-Fe-B Sintered Magnets Using XMCD-PEEM Technique
Sukeyoshi YamamotoMitsuharu YonemuraTakanori WakitaKeiki FukumotoTetsuya NakamuraToyohiko KinoshitaYoshio WatanabeFang Zhun GuoMasugu SatoTomoyuki TeraiTomoyuki Kakeshita
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2008 Volume 49 Issue 10 Pages 2354-2359

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Abstract

A combination of X-Ray Magnetic Circular Dichroism and PhotoEmission Electron Microscopy (XMCD-PEEM) was applied to the magnetic domain analysis of Nd-Fe-B sintered magnets. The XMCD-PEEM high-resolution images revealed both the magnetic domain structures and the microstructural morphologies. In the thermally demagnetized state, each grain in a polycrystalline sample exhibits a multi-domain structure, which is magnetically coupled across grain boundaries. After the DC field-demagnetization, it changed to a single domain structure. The magnetization vector in each surface grain reversed to the negative direction during the field-demagnetization procedure because of the small coercivity in the surface region. In the present study, we observed this surface domain reversal for the first time by means of XMCD-PEEM imaging method, which is important in order to understand the surface phenomena of Nd-Fe-B magnets.

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© 2008 The Japan Institute of Metals and Materials
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